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Beilstein J. Org. Chem. 2018, 14, 2366–2374, doi:10.3762/bjoc.14.212
Graphical Abstract
Scheme 1: (a) Our previously reported Cp*Co(III) redox-neutral coupling of 3-buten-2-one to benzamides, (b) p...
Scheme 2: Summary of reaction conditions optimisation.
Scheme 3: Substrate scope of Cp*Co(III)-catalysed coupling of 3-buten-2-one with functionalised acetanilides....
Figure 1: Mechanistic pathway for Cp*Co(III)-catalysed alkylation of acetanilide with 3-buten-2-one obtained ...
Figure 2: Comparison between energies during the Cp*Co(III)-catalysed coupling of 3-buten-2-one with acetanil...
Figure 3: Comparative visualisation of bcp for Int 2ketone with the acetanilide (left) and benzamide substrat...
Scheme 4: Competitive experiment between coupling to acetanilide (ring A) or benzamide (ring B). aMajor produ...